In this paper, Mn-Fe bimetallic nanoparticles were synthesized by simultaneous reduction of a salt mixture of KMnO4 and FeCl3 with glucose as a reducing agent. Degradation of methyl orange in aqueous solution, using hydrogen peroxide as an oxidizing agent, was used to evaluate the catalytic activity of the material. The material was characterized using scanning electron microscopy, X-ray diffraction, and energy-dispersive X-ray spectroscopy. The results showed that cubic manganese oxide nanoparticles were formed at the molar ratio of KMnO4/C6H12O6·H2O = 5/5 and the hydrothermal temperature of 120-220°C, while the oval-shaped structure was formed at the molar ratio of KMnO4/C6H12O6·H2O = 5/40 and the hydrothermal temperature of 220 °C. The cubic Mn-Fe bimetallic nanoparticle was still formed at the molar ratio of Mn/Fe/C6H12O6 = 5/2/5 and the hydrothermal temperature of 120°C, and the methyl orange decomposition efficiency was found to be the highest value of 57% on this catalyst sample.

In recent years, asymmetric gold nanoparticles have attracted a lot of attention from researchers owing to their unique properties and varied applications in many fields. In this study, gold nanobranches were prepared using a one-step, green reducing method, with the HEPES buffer acting as both a reducing agent and surfactant. The formation of gold nanoparticles was evaluated using UV-Vis spectroscopy by controlling several practical factors, including the volume of gold salt precursor, the concentration of HEPES buffer, and the solution pH. The morphologies and crystallization of the gold nanobranches were characterized by Scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results indicated that under the optimal synthesis conditions, namely 250 µL of 5 mM HAuCl₄, 0.10 M HEPES, and a pH of 7.5, most of the gold particles in the colloidal solution exhibited multiple branches, with an average size ranging from 20 to 35 nm and high crystal density. This study presented a simple synthesis method utilizing eco-friendly substances to replace conventional reducing agents, contributing to the sustainable development of nanotechnology.

Improving and exploring the photocatalytic performance of composites for new models continues to pose a challenge. Here, a straightforward thermal dispersion method is achieved by incorporating nitrogen (N) into TiO2 at different weights (1%, 3%, and 5%) to enhance photocatalytic activity. The material properties are analyzed through ultraviolet-visible diffuse reflectance spectroscopy (UV-VIS DRS), and X-ray diffraction (XRD). The results indicate that the NO gas removal efficiency of N-TiO2 photocatalytic materials is higher than that of pure TiO2 after 30 minutes of exposure to visible light. The highest NO gas treatment efficiency of N-TiO2 -1% is 40.4%, with a reaction rate following a first-order kinetic equation of 0.0688 min-1. Successfully fabricating N-TiO2 photocatalytic materials using the thermal dispersion method, with significantly enhanced photocatalytic performance under visible light activation, will benefit practical applications, particularly in the environmental sector.

Advanced materials have been of interest in recent years because of their outstanding properties that bring many useful applications to humans, they can be highly compatible with alternative materials. In particular, coating materials on HAp base increase the biocompatibility of HAp. In this study, we synthesize TiO2/HAp composite materials using the sol - gel method. Samples were made under different synthesis conditions in terms of HAp/TTIP ratios: (1:1); (1:1.5); (1:2); (1:2.5); (1:3). Factors affecting the synthesis process, such as the incubation time and pH of the solution, were also investigated. The optimal conditions for the synthesis process are the ratio HAp/TTIP: 1 gram HAp with 2 ml TTIP; stirring time: 16 hours; pH of the gel solution: pH = 0.5, as determined from the analysis of the X-ray diffraction spectrum and SEM surface morphology. The research results are the basis for research on biomedical materials.

In this paper, MIL-53(Al) was synthesized by solvothermal method and its application as an adsorbent to remove rhodamine B from aqueous solution. The material was characterized using X-ray diffraction, Fourier-transform infrared spectroscopy, nitrogen adsorption-desorption isotherms, and scanning electron microscopy. The results show that the material has a large specific surface area (1028.3 m2/g). The rhodamine B adsorption on MIL-53(Al) occurs very quickly in the first minutes of contact. Two pseudo-first order and pseudo-second order adsorption kinetic models, and two adsorption isotherm models, including Langmuir and Freundlich, were used to analyze the adsorption data.